Production of hydroxyl radicals in contracting skeletal muscle of cats. O'neill, Charles A., Charles L. Stebbins, Stefanie Bonigut, Barry Halliwell, and John C. Longhurst. Department of Internal Medicine, Division of Cardiovascular Medicine and Department of Human Physiology, University of California, Davis, Davis, CA 95616
APStracts 3:0271A, 1996.
Production of reactive oxygen species (ROS) and indices of oxidative damage appear to increase during exhaustive contraction of skeletal muscle but characterization of the specific species involved and their rates of production during nonexhaustive muscle contraction have not been investigated. Therefore, we tested the hypothesis that the rate of production of hydroxyl radical (HO x ) increases in contracting muscle and that this rate is attenuated by pretreatment with the iron chelator, deferoxamine (DEF), or the nonspecific free radical scavenger, dimethylthiourea (DMTU). We measured the rate of production of HO x before, during, and after 5 min of intermittent static contraction of the triceps surae muscles in cats (n=6). As an index of HO x production, we assessed formation of p-, m- and o -tyrosines by hydroxylation of phenylalanine. L-Phenylalanine (30 mg/kg, intravenous, [iv]) was administered to each animal 3 min before contraction. Blood samples were collected from the popliteal vein 1 min before contraction; 1, 3 and 4.5 min during contraction; and 1 min after contraction. During and following contraction, the cumulative rates of production of p-, m- and o-tyrosines were elevated by 42.84+/-5.41, 0.25+/-0.04 and 0.21+/-0.03 nmol x min-1 x g-1, respectively, compared to production in noncontracting triceps surae muscles. All tyrosines began to increase during early exercise, before the onset of fatigue. The highest rate of production of tyrosines was at 4.5 min of contraction and returned toward precontraction control levels by 1 min after contraction. Pretreatment with DEF (10 mg/kg, iv, n=5) decreased the cumulative rates of production of p-, m- and o-tyrosines during and after contraction by 54+/-8, 22+/-4 and 46+/-7% of control values, respectively. Similarly, pretreatment with DMTU (10 mg/kg, iv, n=4) attenuated the cumulative rates of production of p-, m- and o -tyrosines during and after contraction to 57+/-8, 49+/-11 and 38+/ -7%, respectively. Additionally, D-phenylalanine was administered in a group of seven animals following the same protocol. The cumulative rates of production of p-, m- and o-tyrosines increased by 2.25+/ -0.36, 0.29+/-0.05 and 0.26+/-0.02 nmol x min-1 x g-1, respectively. Finally, the rate of production of tyrosines increased in proportion to the percentage of maximal tension developed by the triceps surae muscles. These results directly demonstrate that HO x is produced in vivo in the skeletal muscle of cats during intermittent static contraction and that this production can occur before the onset of fatigue.

Received 23 October 1995; accepted in final form 3 June 1996.
APS Manuscript Number A1140-5.
Article publication pending Journal of Applied Physiology.
ISSN 1080-4757 Copyright 1996 The American Physiological Society.
Published in APStracts on 28 June 96