The effect of atp-induced permeabilization on loading of the na+ probe, sbfi, into endothelial cells. Cutaia, Michael, Ryan Davis, Nancy Parks, Sharon Rounds. Providence VA Medical Center, Pulmonary Disease Division, Department of Medicine, Brown University School of Medicine, Providence, R.I., 02908
APStracts 3:0122A, 1996.
The fluoroprobe, sodium-binding benzofuran isophthalate (SBFI), is used to measure intracellular cytosolic sodium concentration [Nai]. A problem with the use of this probe is the difficulty in loading it into cells. ATP reversibly increases membrane permeability of some cells via activation of ATP4- receptors. We investigated the effect of ATP-induced membrane permeabilization on loading of the acetoxymethyl ester form of SBFI (SBFI/AM) into bovine pulmonary artery endothelial cells (BPAEC). Monolayers were incubated in a series of solutions which reversibly opened pores, loaded the fluoroprobe, and finally sealed the pores. ATP (1-5mM) or 3'-O-(4 -Benzoyl)benzoyl- adenosine 5'-triphosphate (BzATP; 0.1-1mM), an analogue 30-100x more specific for ATP4- receptors, were utilized to permeabilize the cell membrane. The signal/background ratio (S/B) of the intracellular SBFI fluorescent signal was used as an indicator of the effectiveness of dye loading. ATP and BzATP significantly increased the S/B ratio compared to the values obtained using the standard dye-loading procedure without ATP, indicating that permeabilization increased SBFI/AM entry into cells. The permeabilization procedure produced a small decrease in cell viability, as determined with a fluorescent viability assay (ethidium dimer uptake), compared to the standard method of loading SBFI/AM. We used the procedure to measure baseline [Nai] and changes in [Nai] following the administration of ouabain (10-4M) and monensin (10-5M). Baseline [Nai] with this procedure (19.7+/- 2.7mM; n=15 monolayers) was similar to measurements made in other cell types with the standard method of loading the probe. We conclude: 1) the ATP-induced permeabilization technique is an improved dye-loading method for SBFI/AM in endothelial cell monolayers which facilitates measurement of [Nai]; and 2) these data suggest the presence of an ATP4- pore -forming mechanism in this cell type.

Received 1 June 1995; accepted in final form 14 February 1996.
APS Manuscript Number A571-5.
Article publication pending Journal of Applied Physiology.
ISSN 1080-4757 Copyright 1996 The American Physiological Society.
Published in APStracts on 13 March 96